Crystals

Recently I've been playing around with growing crystals. It was always a fun and easy thing to do when I was a kid, so I thought I'd try some that are more interesting than the usual salt, sugar, alum, epsom, etc. This is recrystalized acetylsalicylic acid, asprin, from OTC tablets. 10g pulverized, washed with cold water, vacuum filtered, then dissolved in 250mL of 75C water and allowed to cool slowly. Crystals approximately 3-5 mm in length. I will chill this and allow crystal formation to finish, then wash the crystals and recrystallize at a slower rate.
This is benzocaine, extracted from Oragel tooth gel. 0.5g of gel stirred in 15mL cold water until dissolved. Benzoncaine will form white flakes. Centrifuge and draw off supernatant. Add 20mL water and heat in hot water bath. A bead of molten benzocaine will form. Add sufficient water to dissolve the bead. Allow to cool and crystallize. Vacuum filter and collect for recrystallization.
This is what I think is probably salicyclic acid. 1g of OTC tablets, pulverized, heated in 20mL water until dissolved. When cooled the entire 20mL formed one huge crystal block, which was amusing. Melted again, added 10mL water and heated until acetic acid formed. Cooling produced fine, hair-like crystals, which I suspect are salicyclic acid (more research to do). Washed and vacuum filtered, will recrystallize to see if more pure crystals look different.

Leave a Reply

Your email address will not be published. Required fields are marked *